HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66723718, compound → HCID 131732786, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66723718 | HCID 66723718 | — |
| Reactant | HCID 131732785 | HCID 131732785 | — |
| Product | HCID 131732786 | HCID 131732786 | 77% |
Reaction Steps
The title product (1.2 g, yield: 77%) was prepared using a procedure similar to the one described for the synthesis of INTERMEDIATE 103. (R)-tert-Butyl 3-((tert-butyldiphenylsilyloxy)methyl)morpholine-4-carboxylate (INTERMEDIATE 106, 2.0 g, 4.39 mmol) was used as starting material. The title product was obtained as a hydrochloride salt after evaporation of the volatiles under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09248140B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-0a7b35ebbd7340bc9215a9611d18ffd0 |
| Source note | uspto-grants-2016_02 |