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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1771221Generated: October 30, 2026

HCID 66723718, compound → HCID 131732786, compound

https://huagongshe.com/reaction/1771221

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 66723718HCID 66723718—
ReactantHCID 131732785HCID 131732785—
ProductHCID 131732786HCID 13173278677%

Reaction Steps

The title product (1.2 g, yield: 77%) was prepared using a procedure similar to the one described for the synthesis of INTERMEDIATE 103. (R)-tert-Butyl 3-((tert-butyldiphenylsilyloxy)methyl)morpholine-4-carboxylate (INTERMEDIATE 106, 2.0 g, 4.39 mmol) was used as starting material. The title product was obtained as a hydrochloride salt after evaporation of the volatiles under reduced pressure.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09248140B2
Source datasetuspto-grants-2016_02
ORD IDord-0a7b35ebbd7340bc9215a9611d18ffd0
Source noteuspto-grants-2016_02