Cupric acetate → 14167-15-8
Reaction equation
[CH:1]1[CH:20]=[CH:19][C:17](=[O:18])/[C:3](=[CH:4]/[NH:5][CH2:6][CH2:7][NH:8]/[CH:9]=[C:10]2/[CH:11]=[CH:12][CH:13]=[CH:14][C:15]/2=[O:16])/[CH:2]=1.CC([O-])=O.CC([O-])=O.[Cu+2:29]>C(O)C>[CH:12]1[CH:11]=[C:10]([CH:9]=[N:8][CH2:7][CH2:6][N:5]=[CH:4][C:3]2[C:17]([O-:18])=[CH:19][CH:20]=[CH:1][CH:2]=2)[C:15]([O-:16])=[CH:14][CH:13]=1.[Cu+2:29]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Conditions
- Temperature
- 80 °C
Procedure
Anhydrous ethanol was added to a mixture of Salen and Cu(OAc)2 under argon via a syringe. The reaction mixture was stirred at 80° C. for 24 hours. The solvent was removed under reduced pressure, yielding a dark green powder Salen-Cu.
Workup
- customThe solvent was removed under reduced pressure
Sources & evidence
- ORD record
- ord-1dcd57c0b38645ca81ed059274ba572a
- Source dataset
- uspto-grants-2016_02
- Patent number
- US09249120B2
Reaction notes
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