Cupric acetate → 14167-15-8

HRID 1771261Notes

Reaction equation

HRID 1771261 reaction equation
CC([O-])=O.CC([O-])=O.[Cu+2:9].[CH:10]1[CH:29]=[CH:28][C:26](=[O:27])/[C:12](=[CH:13]/[NH:14][CH2:15][CH2:16][NH:17]/[CH:18]=[C:19]2/[CH:20]=[CH:21][CH:22]=[CH:23][C:24]/2=[O:25])/[CH:11]=1>C(O)C>[CH:21]1[CH:20]=[C:19]([CH:18]=[N:17][CH2:16][CH2:15][N:14]=[CH:13][C:12]2[C:26]([O-:27])=[CH:28][CH:29]=[CH:10][CH:11]=2)[C:24]([O-:25])=[CH:23][CH:22]=1.[Cu+2:9]

Participants

4

Reactant 2

HCID 8895Cupric acetateHCID 178515945HCID 178515945, compound

Product 1

HCID 1254462114167-15-8

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Conditions

Temperature
80 °C

Procedure

The Cu(OAc)2 (0.5 mmol) and Salen (N′N′-bis(3-tert-butyl-5-bromo-salicylidene)-1,2-diaminocyclohexane, 0.5 mmol) and were dissolved in dried ethanol (20 mL). The mixture was stirred at 80° C. for 24 hours. After that the compound Salen-Cu was obtained.

Sources & evidence

ORD record
ord-c70085b7618d4b20a685e17d10c8b39c
Source dataset
uspto-grants-2016_02
Patent number
US09249120B2

Reaction notes

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