HuagongsheHuagongshe Chemistry Print Report · For research reference only
Selenium Dioxide → 146535-00-4
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Selenium Dioxide | HCID 24007 | — |
| Reactant | 3',5'-Difluoroacetophenone | HCID 518596 | — |
| Product | 146535-00-4 | HCID 18784701 | 85.6% |
Reaction Steps
(3,5-Difluorophenyl)(oxo)acetaldehyde (28 g, 84%) was prepared from 3,5-difluoro acetophenone (30.0 g, 192.3 mmol) and selenium dioxide (23.55 g, 214.0 mmol) according to the typical procedure used for Preparation 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249130B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-060a619f5ae64f888d1bb22a131848f1 |
| Source note | uspto-grants-2016_02 |