HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Acetylpyridine → 3-PYRIDINEACETALDEHYDE, ALPHA-OXO-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Acetylpyridine | HCID 9589 | — |
| Reactant | Selenium Dioxide | HCID 24007 | — |
| Product | 3-PYRIDINEACETALDEHYDE, ALPHA-OXO- | HCID 10236008 | 90.3% |
Reaction Steps
3-Pyridylglyoxal (5.0 g, crude) was prepared from selenium dioxide (6.82 g, 61.4 mmol) and 3-acetyl pyridine (5.0 g, 41.0 mmol) according to the typical procedure used for Preparation 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249130B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-25bdcaca6c53457195631dffd3302413 |
| Source note | uspto-grants-2016_02 |