HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorophenylglyoxal hydrate → 5-(4-Fluoro-phenyl)-3-methylsulfanyl-[1,2,4]triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorophenylglyoxal hydrate | HCID 2737470 | — |
| Reactant | Methyl hydrazinecarbimidothioate | HCID 178504051 | — |
| Product | 5-(4-Fluoro-phenyl)-3-methylsulfanyl-[1,2,4]triazine | HCID 654246 | 69% |
Reaction Steps
3-(Methylsulfanyl)-5-(4-fluorophenyl)-1,2,4-triazine (6.00 g, 69%) was prepared from methyl hydrazinecarbimidothioate (4.51 g, 43.0 mmol) and 4-fluorophenylglyoxal monohydrate (6.60 g, 43.0 mmol) according to the general procedure of Preparation 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249130B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-c5f953ae782c4214968f1707bf7ab0f4 |
| Source note | uspto-grants-2016_02 |