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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1771380Generated: November 2, 2026

N-Iodosuccinimide → HCID 136333900, compound

https://huagongshe.com/reaction/1771380

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN-IodosuccinimideHCID 120273—
ReactantHCID 136333901HCID 136333901—
SolventAcetic AcidHCID 176—
ProductHCID 136333900HCID 136333900—

Reaction Steps

4-(3-Amino-5-phenyl-1,2,4-triazin-6-yl)-phenol (vide supra; 140 mg, 0.530 mmol) was reacted with AcOH (2 mL) and 1-iodopyrrolidine-2,5-dione (119 mg, 0.530 mmol). The mixture was stirred at room temperature for 1 hour then concentrated in vacuo and purified by column chromatography (35 mg, 32%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09249130B2
Source datasetuspto-grants-2016_02
ORD IDord-0a135a0611be431b9c71ab48be65f49d
Source noteuspto-grants-2016_02