Ozone → HCID 89851711, compound

Participants

Reaction Steps

To a solution of 1-(2-(benzyloxy)pent-4-enyl)-2-methylbenzene (5.0 g, 18.72 mmol) in DCM (100 ml) was passed O3 gas at −78° C. for 3 h. The reaction mixture was quenched with TEA (5 ml) at −78° C., and stirred for room temperature for 5 h. The title compound was purified by separation methods A and E. (Yield 2.0 g).

Provenance & Evidence