HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Carboxyphenylboronic Acid → HCID 57387163, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Carboxyphenylboronic Acid | HCID 312183 | — |
| Reactant | 6-Bromo-1-fluoronaphthalen-2-OL | HCID 11241940 | — |
| Product | HCID 57387163 | HCID 57387163 | — |
Reaction Steps
Followed the coupling procedure described in Example 29 starting from 6-bromo-1-fluoronaphthalen-2-ol (Intermediate 13) and 4-boronobenzoic acid. 1H-NMR (DMSO-d6, 300 MHz, TMS): δ 13.04 (b, 1H), 10.23 (b, 1H), 8.29 (s, 1H), 7.91-8.01 (m, 7H), 7.74 (d, 1H). MS (ESI): m/z=281.26 [M−1]−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249132B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-8dd0a9f07fa64f6a863948c061d9cbad |
| Source note | uspto-grants-2016_02 |