HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propenoic acid, 3-phenyl- → 3-Phenylprop-2-enoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propenoic acid, 3-phenyl- | HCID 8784 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 3-Phenylprop-2-enoyl chloride | HCID 66023 | — |
Reaction Steps
Cinnamic acid (25 g, 168.74 mmol) was treated with SOCl2 (150 ml) for 2 hours at 70° C. in a round-bottomed flask. The volatiles were distilled out under vacuum to afford cinnamoyl chloride as a yellow oil (25.2 g, crude), which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249102B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-1ccd6a242fb34c7dab61a725dbd1c561 |
| Source note | uspto-grants-2016_02 |