HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1772233Generated: November 1, 2026
Allyl bromide → 1-Fluoro-4-(prop-2-en-1-yloxy)benzene
https://huagongshe.com/reaction/1772233
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | 4-Fluorophenol | HCID 9732 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 1-Fluoro-4-(prop-2-en-1-yloxy)benzene | HCID 637342 | — |
Reaction Steps
Into a 1 L round-bottomed flask containing 500 ml of acetonitrile was added 4-fluorophenol (30.0 g, 267.6 mmol), 3-bromoprop-1-ene (41.7 g, 344.7 mmol, 1.3 eq), and potassium carbonate (55 g, 398 mmol, 1.5 eq). The mixture was stirred for 3.5 hours at 60° C. (oil bath).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09249102B2 |
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| Source dataset | uspto-grants-2016_02 |
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| ORD ID | ord-a54d41b5cad94f48bb105897c5e38415 |
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| Source note | uspto-grants-2016_02 |
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