HCID 86624786, compound → HCID 44628665, compound

Participants

Reaction Steps

7l was synthesized from 6g as described for 6a. White lyophilised powder. Molecular Formula C13H13FN4O3. 1H NMR (DMSO-d6, 400 MHz) δ (ppm) 3.61 (d, J=5.52 Hz, 1H), 3.63-3.67 (m, 1H), 3.80-3.83 (d, J=12.14 Hz, 1H), 3.86-3.88 (d, J=9.38 Hz, 1H), 4.46-4.54 (dd, J=23.23 Hz and J=9.39 Hz, 1H), 5.30 (brs, 1H), 6.1 (brs, 1H), 6.41-6.47 (d, J=16.47 Hz, 1H), 6.57-6.61 (d, J=16.47 Hz, 1H), 7.04 (s, 2H), 7.37-7.38 (d, J=3.65 Hz, 1H), 8.05 (s, 1H) 19F NMR (DMSO-d6, 235 MHz) δ (ppm) −157.15 (s, 1F) Scan ES+ 293 (M+H)+, UV λmax 275 nm

Provenance & Evidence