2-Nitrobenzenesulfonyl chloride → HCID 3860390, compound

HRID 1772852Notes

Reaction equation

HRID 1772852 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[S:10](Cl)(=[O:12])=[O:11])([O-:3])=[O:2].[F:14][C:15]([S:18][C:19]1[CH:20]=[C:21]([CH:23]=[CH:24][CH:25]=1)[NH2:22])([F:17])[F:16]>>[N+:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[S:10]([NH:22][C:21]1[CH:23]=[CH:24][CH:25]=[C:19]([S:18][C:15]([F:17])([F:14])[F:16])[CH:20]=1)(=[O:12])=[O:11])([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 155402-Nitrobenzenesulfonyl chlorideHCID 27359393-((Trifluoromethyl)thio)aniline

Product 1

HCID 3860390HCID 3860390, compoundYield 66%

Procedure

The title compound (1.26 g, 3.3 mmol) was prepared from 2-nitrobenzenesulfonyl chloride (1.1 g, 5.0 mmol) and 3-[(trifluoromethyl)sulfanyl]aniline (1.06 g, 5.5 mmol) using the methods of (IntA1), step 1.

Sources & evidence

ORD record
ord-1049cb4f6aa54070b87250df96e40eb0
Source dataset
uspto-grants-2016_02
Patent number
US09249160B2

Reaction notes

Loading…