HCID 26970545, compound → HCID 16785511, compound

HRID 1772856Notes

Reaction equation

HRID 1772856 reaction equation
[CH3:1][O:2][C:3]1[N:8]=[CH:7][C:6]([NH:9][S:10]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=2[N+:19]([O-])=O)(=[O:12])=[O:11])=[CH:5][CH:4]=1>[Pd]>[NH2:19][C:14]1[CH:15]=[CH:16][CH:17]=[CH:18][C:13]=1[S:10]([NH:9][C:6]1[CH:7]=[N:8][C:3]([O:2][CH3:1])=[CH:4][CH:5]=1)(=[O:11])=[O:12]

Participants

3

Reactant 1

HCID 26970545HCID 26970545, compound

Product 1

HCID 16785511HCID 16785511, compoundYield 92.6%

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

The title compound (419 mg 1.50 mmol) was prepared from N-(6-Methoxypyridin-3-yl)-2-nitrobenzenesulfonamide (500 mg, 1.62 mmol) and 10% palladium on charcoal (50 mg) using the methods of (IntA14), step 2.

Sources & evidence

ORD record
ord-5823163036bb420fb62dc9a9544030bd
Source dataset
uspto-grants-2016_02
Patent number
US09249160B2

Reaction notes

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