HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 90055163, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 16785511 | HCID 16785511 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 90055163 | HCID 90055163 | 62.7% |
Reaction Steps
The title compound (143 mg, 0.47 mmol) was prepared from 2-amino-N-(6-methoxypyridin-3-yl)benzenesulfonamide (209 mg, 0.75 mmol), 1,1′-carbonyldiimidazole (486 mg, 3.0 mmol) and triethylamine (0.28 mL, 1.5 mmol) in DMF (3.75 mL) using the methods of (IntA14), step 3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249160B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-eb2e68fa84fa49a08751c7201c8903fa |
| Source note | uspto-grants-2016_02 |