HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous Chloride → 2-amino-4-fluoro-N-[3-(methylsulfanyl)phenyl]benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | 4-fluoro-N-[3-(methylsulfanyl)phenyl]-2-nitrobenzenesulfonamide | HCID 26952414 | — |
| Product | 2-amino-4-fluoro-N-[3-(methylsulfanyl)phenyl]benzenesulfonamide | HCID 29268434 | 98.8% |
Reaction Steps
The title compound (780 mg, 2.50 mmol) was prepared from 4-fluoro-N-[3-(methylsulfanyl)phenyl]-2-nitrobenzenesulfonamide (865 mg, 2.53 mmol) and SnCl2 (1.44 g, 7.59 mmol) using the methods of (IntA1), Step 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249160B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-b56b9b41823243ff8424867673c11cce |
| Source note | uspto-grants-2016_02 |