HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(5,6-Dimethoxypyridin-3-yl)-2-nitrobenzenesulfonamide → 2-amino-N-(5,6-dimethoxypyridin-3-yl)benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(5,6-Dimethoxypyridin-3-yl)-2-nitrobenzenesulfonamide | HCID 118045902 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 2-amino-N-(5,6-dimethoxypyridin-3-yl)benzenesulfonamide | HCID 90021791 | 104.7% |
Reaction Steps
The title compound (486 mg) was prepared from N-(5,6-dimethoxypyridin-3-yl)-2-nitrobenzenesulfonamide (509 mg, 1.5 mmol), Fe powder (559 mg, 15.0 mmol) and acetic acid (10 mL) using the methods of (IntA17), Step 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249160B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-5cfe7d8b8d9c4e28a05b5cda7673ad65 |
| Source note | uspto-grants-2016_02 |