Potassium Carbonate → 2-(3,4-Dimethoxyphenyl)-4-(2,4,6-trifluorobenzyl)-2H-1,2,4-benzothiadiazin-3(4H)-one 1,1-dioxide

참여 물질

역할	이름	HCID	투입량
반응물	Potassium Carbonate	HCID 11430	—
반응물	2,4,6-Trifluorobenzyl bromide	HCID 2777059	—
반응물	2-(4-methoxy-3,5-dimethylphenyl)-4-(2,4,6-trifluorobenzyl)-2H-1,2,4-benzothiadiazin-3(4H)-one 1,1-dioxide	HCID 72722085	—
용매	Dimethylformamide	HCID 6228	—
생성물	2-(3,4-Dimethoxyphenyl)-4-(2,4,6-trifluorobenzyl)-2H-1,2,4-benzothiadiazin-3(4H)-one 1,1-dioxide	HCID 72721795	—

반응 단계

The title compound (29 mg, 0.06 mmol) was prepared from (IntA1) (84 mg, 0.25 mmol), K2CO3 (104 mg, 0.75 mmol) and 2,4,6-trifluorobenzyl bromide (68 uL, 0.30 mmol) in DMF (2 mL) using the methods of (115).

출처 및 근거

DOI	10.6084/m9.figshare.5104873.v1
특허 번호	US09249160B2
출처 데이터셋	uspto-grants-2016_02
ORD ID	ord-a6b850497dc0481e9819efeb59613c32
출처 메모	uspto-grants-2016_02