Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1773522Generated: November 1, 2026

4-ethenyl-1-methoxy-2-nitrobenzene → 5-Ethyl-2-methoxyaniline

https://huagongshe.com/reaction/1773522

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-ethenyl-1-methoxy-2-nitrobenzeneHCID 244416—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
Product5-Ethyl-2-methoxyanilineHCID 22065596—

Reaction Steps

A mixture of 1-methoxy-2-nitro-4-vinyl-benzene (150 mg) and palladium on carbon (10%, 25 mg) in ethyl acetate (10 mL) was stirred under hydrogen atmosphere (balloon pressure) at room temperature overnight. The reaction mixture was filtered on a CELITE™ pad and the filtrate was evaporated to give 5-ethyl-2-methoxy-phenylamine without further purifications.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09255110B2
Source datasetuspto-grants-2016_02
ORD IDord-0c13ada629df41f995fb376f20e1468b
Source noteuspto-grants-2016_02