HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-ethenyl-1-methoxy-2-nitrobenzene → 5-Ethyl-2-methoxyaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-ethenyl-1-methoxy-2-nitrobenzene | HCID 244416 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 5-Ethyl-2-methoxyaniline | HCID 22065596 | — |
Reaction Steps
A mixture of 1-methoxy-2-nitro-4-vinyl-benzene (150 mg) and palladium on carbon (10%, 25 mg) in ethyl acetate (10 mL) was stirred under hydrogen atmosphere (balloon pressure) at room temperature overnight. The reaction mixture was filtered on a CELITE™ pad and the filtrate was evaporated to give 5-ethyl-2-methoxy-phenylamine without further purifications.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09255110B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-0c13ada629df41f995fb376f20e1468b |
| Source note | uspto-grants-2016_02 |