4-Acetamidophenylboronic acid → HCID 24810712, compound

HRID 1774115Notes

Reaction equation

HRID 1774115 reaction equation
[NH2:1][C:2]1[N:11]=[C:10]([NH:12][CH:13]2[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]2)[C:9]2[C:4](=[CH:5][CH:6]=[C:7](Br)[CH:8]=2)[N:3]=1.[C:20]([NH:23][C:24]1[CH:29]=[CH:28][C:27](B(O)O)=[CH:26][CH:25]=1)(=[O:22])[CH3:21]>>[NH2:1][C:2]1[N:11]=[C:10]([NH:12][CH:13]2[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]2)[C:9]2[C:4](=[CH:5][CH:6]=[C:7]([C:27]3[CH:28]=[CH:29][C:24]([NH:23][C:20](=[O:22])[CH3:21])=[CH:25][CH:26]=3)[CH:8]=2)[N:3]=1

Participants

3

Reactant 2

HCID 27346574-Acetamidophenylboronic acidHCID 24810155HCID 24810155, compound

Product 1

HCID 24810712HCID 24810712, compoundYield 95%

Procedure

This compound was synthesized from the product of example 20 and 4-acetamidophenyl-boronic acid, in 95% yield, using the procedure described for example 7, and was characterized by its mass spectrum as follows: MS (m/z): 376 ([M+H]+, 100).

Sources & evidence

ORD record
ord-de3d1105a3494d678db4304bbca26df2
Source dataset
uspto-grants-2016_02
Patent number
US09259426B2

Reaction notes

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