HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloropinacolone → 1-(3,3-Dimethyl-2-oxobutyl)-3-mesityl imidazolium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloropinacolone | HCID 83572 | — |
| Reactant | 1-Mesityl-1h-imidazole | HCID 9815460 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1-(3,3-Dimethyl-2-oxobutyl)-3-mesityl imidazolium chloride | HCID 86653161 | — |
Reaction Steps
According to the general synthesis procedure, 5.4 mmol (1.00 g) 1-mesitylimidazole and 6.4 mmol (0.870 g, 0.85 ml) 1-chloro-3,3-dimethyl-2-butanone are dissolved in 5 ml THF and heated for 45 min to 90° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09260397B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-e2e7e09c5fa24ceb9ab565b4b33dba98 |
| Source note | uspto-grants-2016_02 |