1-Bromohexane → HCID 178444692, compound

HRID 1774347Notes

Reaction equation

HRID 1774347 reaction equation
[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[N:10]1[CH:14]=[CH:13][N:12]=[CH:11]1)[CH3:2].[Br:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]>C(OCC)C>[Br-:15].[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[N+:10]1[CH:14]=[CH:13][N:12]([CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21])[CH:11]=1)[CH3:2]

Participants

4

Reactant 2

HCID 81011-BromohexaneHCID 58249724HCID 58249724, compound

Product 1

HCID 178444692HCID 178444692, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

According to the general synthesis procedure, 10.00 mmol (1,883 g) 1-(2-ethoxyphenyl)imidazole and 11.00 mmol (1,816 g, 1.59 ml) 1-bromohexane are dissolved in 3 ml diethylether and heated for 12 h to 60° C.

Workup

  1. temperatureheated for 12 h to 60° C.

Sources & evidence

ORD record
ord-9685deeb357643c7bfb573601752e1fd
Source dataset
uspto-grants-2016_02
Patent number
US09260397B2

Reaction notes

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