1-Bromoheptane → HCID 178444696, compound

HRID 1774349Notes

Reaction equation

HRID 1774349 reaction equation
[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][C:7]([N:10]2[CH:14]=[CH:13][N:12]=[CH:11]2)=[CH:6][CH:5]=1)[CH3:2].[Br:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21]C>C(OCC)C>[Br-:15].[CH2:1]([O:3][C:4]1[CH:5]=[CH:6][C:7]([N+:10]2[CH:14]=[CH:13][N:12]([CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21])[CH:11]=2)=[CH:8][CH:9]=1)[CH3:2]

Participants

4

Reactant 2

HCID 123691-BromoheptaneHCID 3028816HCID 3028816, compound

Product 1

HCID 178444696HCID 178444696, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

According to the general synthesis procedure, 10.00 mmol (1,883 g) 1-(4-ethoxyphenyl)imidazole and 11.00 mmol (1,816 g, 1.59 ml) 1-bromoheptane are dissolved in 3 ml diethylether and heated for 12 h to 60° C.

Workup

  1. temperatureheated for 12 h to 60° C.

Sources & evidence

ORD record
ord-00b6692fa16e4292a28cb03b13e4b9d2
Source dataset
uspto-grants-2016_02
Patent number
US09260397B2

Reaction notes

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