Ammonium hexafluorophosphate → HCID 86653213, compound

HRID 1774357Notes

Reaction equation

HRID 1774357 reaction equation
[Br-].[CH2:2]([N+:4]1[CH:8]=[CH:7][N:6]([C:9]2[C:14]([CH3:15])=[CH:13][C:12]([CH3:16])=[CH:11][C:10]=2[CH3:17])[CH:5]=1)[CH3:3].[F:18][P-:19]([F:24])([F:23])([F:22])([F:21])[F:20].[NH4+]>O>[F:18][P-:19]([F:24])([F:23])([F:22])([F:21])[F:20].[CH2:2]([N+:4]1[CH:8]=[CH:7][N:6]([C:9]2[C:14]([CH3:15])=[CH:13][C:12]([CH3:16])=[CH:11][C:10]=2[CH3:17])[CH:5]=1)[CH3:3]

Participants

4

Reactant 2

HCID 9793912Ammonium hexafluorophosphateHCID 86653212HCID 86653212, compound

Product 1

HCID 86653213HCID 86653213, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

According to the general synthesis procedure, 1.18 mmol (0.380 g) 1-ethyl-3-mesityl imidazolium bromide and 1.30 mmol (0.212 g) ammonium hexafluorophosphate are dissolved in 4 ml water. The immediately produced white precipitate is extracted with dichloromethane, the organic phase is dried over magnesium sulfate, and the solvent is removed in vacuum.

Workup

  1. extractionThe immediately produced white precipitate is extracted with dichloromethane
  2. dry with materialthe organic phase is dried over magnesium sulfate
  3. customthe solvent is removed in vacuum

Sources & evidence

ORD record
ord-8aa2362cf6524c18b01a5424d9ace87b
Source dataset
uspto-grants-2016_02
Patent number
US09260397B2

Reaction notes

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