Ammonium hexafluorophosphate → HCID 86653221, compound

HRID 1774358Notes

Reaction equation

HRID 1774358 reaction equation
[Br-].[CH2:2]([N+:8]1[CH:12]=[CH:11][N:10]([C:13]2[C:18]([CH3:19])=[CH:17][C:16]([CH3:20])=[CH:15][C:14]=2[CH3:21])[CH:9]=1)[CH2:3][CH2:4][CH2:5][CH2:6][CH3:7].[F:22][P-:23]([F:28])([F:27])([F:26])([F:25])[F:24].[NH4+]>O.CO>[F:22][P-:23]([F:28])([F:27])([F:26])([F:25])[F:24].[CH2:2]([N+:8]1[CH:12]=[CH:11][N:10]([C:13]2[C:18]([CH3:19])=[CH:17][C:16]([CH3:20])=[CH:15][C:14]=2[CH3:21])[CH:9]=1)[CH2:3][CH2:4][CH2:5][CH2:6][CH3:7]

Participants

5

Reactant 2

HCID 9793912Ammonium hexafluorophosphateHCID 86653222HCID 86653222, compound

Product 1

HCID 86653221HCID 86653221, compound

Reagents, catalysts & solvents 2

HCID 887MethanolSolventHCID 962WaterSolvent

Procedure

According to the general synthesis procedure, 1.42 mmol (0.500 g) 1-hexyl-3-mesityl imidazolium bromide and 1.57 mmol (0.260 g) ammonium hexafluorophosphate are dissolved in a mixture of 8 ml water and 2 ml methanol and stirred at room temperature.

Sources & evidence

ORD record
ord-150de515e3e54a5baf988896e7ceda5c
Source dataset
uspto-grants-2016_02
Patent number
US09260397B2

Reaction notes

Loading…