Methanol → HCID 178443588, compound

HRID 1774359Notes

Reaction equation

HRID 1774359 reaction equation
[Br-].[C:2]1([CH3:23])[CH:7]=[C:6]([CH3:8])[CH:5]=[C:4]([CH3:9])[C:3]=1[N+:10]1[CH:14]=[CH:13][N:12]([CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])[CH:11]=1.CO.[F:26][P-:27]([F:32])([F:31])([F:30])([F:29])[F:28].[NH4+]>O>[F:26][P-:27]([F:32])([F:31])([F:30])([F:29])[F:28].[C:4]1([CH3:9])[CH:5]=[C:6]([CH3:8])[CH:7]=[C:2]([CH3:23])[C:3]=1[N+:10]1[CH:14]=[CH:13][N:12]([CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])[CH:11]=1

Participants

5

Reactant 3

HCID 887MethanolHCID 9793912Ammonium hexafluorophosphateHCID 178443587HCID 178443587, compound

Product 1

HCID 178443588HCID 178443588, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

According to the general synthesis procedure, 0.66 mmol (0.252 g) 1-mesityl-3-octyl imidazolium bromide is dissolved in 6 ml water and 3 ml methanol and 0.73 mmol (0.120 g) ammonium hexafluorophosphate is added.

Sources & evidence

ORD record
ord-5b16dd75585a4396a89e5a96236e23fb
Source dataset
uspto-grants-2016_02
Patent number
US09260397B2

Reaction notes

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