m-Chlorophenylhydrazine hydrochloride → HCID 71078131, compound

HRID 1774490Notes

Reaction equation

HRID 1774490 reaction equation
[CH3:1][O:2][C:3](=[O:15])[C:4]1[CH:9]=[CH:8][N:7]=[C:6]([S:10][CH2:11][C:12](=O)[CH3:13])[CH:5]=1.Cl.[Cl:17][C:18]1[CH:19]=[C:20]([NH:24]N)[CH:21]=[CH:22][CH:23]=1>>[CH3:1][O:2][C:3](=[O:15])[C:4]1[CH:9]=[CH:8][N:7]=[C:6]([S:10][C:11]2[C:21]3[C:20](=[CH:19][C:18]([Cl:17])=[CH:23][CH:22]=3)[NH:24][C:12]=2[CH3:13])[CH:5]=1

Participants

3

Reactant 2

HCID 75331m-Chlorophenylhydrazine hydrochlorideHCID 71076611HCID 71076611, compound

Product 1

HCID 71078131HCID 71078131, compound

Procedure

Prepared according to the procedure described in Example 1, Step 4, using the following starting materials: 2-(2-oxo-propylsulfanyl)-isonicotinic acid methyl ester and (3-chloro-phenyl)-hydrazine hydrochloride.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-c653af19d06448f1b48c7f7d49f8cee5
Source dataset
uspto-grants-2016_02
Patent number
US09260416B2

Reaction notes

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