Ethyl 6-Bromopicolinate → HCID 71076558, compound

HRID 1774494Notes

Reaction equation

HRID 1774494 reaction equation
[CH2:1]([O:3][C:4]([C:6]1[CH:11]=[CH:10][CH:9]=[C:8](Br)[N:7]=1)=[O:5])[CH3:2].[CH:13]([Si:16]([CH:21]([CH3:23])[CH3:22])([CH:18]([CH3:20])[CH3:19])[SH:17])([CH3:15])[CH3:14]>>[CH2:1]([O:3][C:4]([C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([S:17][Si:16]([CH:18]([CH3:20])[CH3:19])([CH:21]([CH3:23])[CH3:22])[CH:13]([CH3:14])[CH3:15])[N:7]=1)=[O:5])[CH3:2]

Participants

3

Reactant 2

HCID 2758810Ethyl 6-BromopicolinateHCID 3435097Tris(propan-2-yl)silanethiol

Product 1

HCID 71076558HCID 71076558, compound

Procedure

Prepared according to the procedure described in Example 6, Step 1, using the following starting materials: 6-bromo-pyridine-2-carboxylic acid ethyl ester and triisopropylsilane-thiol.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-de7afd6101914a2582e5850f294d4528
Source dataset
uspto-grants-2016_02
Patent number
US09260416B2

Reaction notes

Loading…