(3-Chloro-2-fluorophenyl)hydrazine--hydrogen chloride (1/1) → HCID 71078006, compound

HRID 1774509Notes

Reaction equation

HRID 1774509 reaction equation
[CH2:1]([O:3][C:4](=[O:16])[CH2:5][N:6]1[CH:10]=[C:9]([S:11][CH2:12][C:13](=O)[CH3:14])[CH:8]=[N:7]1)[CH3:2].Cl.[Cl:18][C:19]1[C:20]([F:27])=[C:21]([NH:25]N)[CH:22]=[CH:23][CH:24]=1>>[CH2:1]([O:3][C:4](=[O:16])[CH2:5][N:6]1[CH:10]=[C:9]([S:11][C:12]2[C:22]3[C:21](=[C:20]([F:27])[C:19]([Cl:18])=[CH:24][CH:23]=3)[NH:25][C:13]=2[CH3:14])[CH:8]=[N:7]1)[CH3:2]

Participants

3

Reactant 2

HCID 25067375(3-Chloro-2-fluorophenyl)hydrazine--hydrogen chloride (1/1)HCID 71076591HCID 71076591, compound

Product 1

HCID 71078006HCID 71078006, compound

Procedure

Prepared according to the procedure described in Example 1, Step 4, using the following starting materials: [4-(2-oxo-propylsulfanyl)-pyrazol-1-yl]-acetic acid ethyl ester and 3-chloro-2-fluorophenylhydrazine hydrochloride.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-b5570acff7fb4a0d99767f1df9953511
Source dataset
uspto-grants-2016_02
Patent number
US09260416B2

Reaction notes

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