P,P-Diphenylphosphinic azide → HCID 71533636, compound

Participants

Reaction Steps

In analogy to the procedure described for the preparation of example 59 [D], 2-methyl-2-(5-(1-methyl-2-oxo-1,2,3,4-tetrahydroquinolin-6-yl)pyridin-3-yl)propanoic acid (example 72 [C]) was reacted with diphenylphosphoryl azide in presence of TEA and then sodium trimethylsilanoate (1 M in THF) to give the title compound as a light brown amorphous solid. MS: 296.5 (M+H+).

Provenance & Evidence