Methylhydrazine → HCID 66576809, compound

HRID 1775535Notes

Reaction equation

[Cl:1][C:2]1[C:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[N:6][N:5]=[C:4]2[NH:14][N:15]=C(C3C=CC=CC=3)[C:3]=12.[CH3:23][C:24]1[CH:31]=[CH:30][CH:29]=[CH:28][C:25]=1[CH:26]=O.[CH3:32]NN>>[Cl:1][C:2]1[C:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[N:6][N:5]=[C:4]2[N:14]([CH3:32])[N:15]=[C:26]([C:25]3[CH:28]=[CH:29][CH:30]=[CH:31][C:24]=3[CH3:23])[C:3]=12

Participants

Reactant 3

HCID 6061Methylhydrazine

HCID 107222-Methylbenzaldehyde

HCID 86697018CID 86697018

Product 1

HCID 66576809HCID 66576809, compound

Procedure

Compound 20 was synthesised following similar procedures outlined in Example 22 (Compound 9), using 2-methylbenzaldehyde instead of benzaldehyde in Step 1 and methyl hydrazine instead of hydrazine hydrate in Step 3.

Sources & evidence

ORD record: ord-9a2db17439814e85968bc60d35e4faf6
Source dataset: uspto-grants-2016_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09260381B2

Reaction notes

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