HCID 86679529, compound → HCID 86679530, compound

Participants

Reaction Steps

2-(benzyloxy)-2-oxoethyl 4-(cyclopropylmethoxy)-3-(morpholinomethyl)-benzoate (4.55 g, 10.35 mmol) was dissolved in MeOH (50 ml), then Pd/C 5% (1.10 g, 0.340 mmol) was added. The solution was shaken under hydrogen atmosphere at 60 psi on a Parr apparatus for 1 hour. The catalyst was filtered off and the solvent removed under vacuum to give 3.18 g of the desired compound (yield 88%).

Provenance & Evidence