HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 43717865, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Methoxy-2-nitroaniline | HCID 66793 | — |
| Reactant | 2-Bromobenzyl bromide | HCID 76965 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 43717865 | HCID 43717865 | — |
Reaction Steps
To a solution of 4-methoxy-2-nitrobenzenamine (16.8 g, 0.1 mol) and 1-bromo-2-(bromomethyl)benzene (30 g, 0.12 mol) in CH3CN (700 mL) was added K2CO3 (27.6 g, 0.2 mol). The mixture was heated to reflux for 60 h then cooled to RT filtered and concentrated to dryness. The resulting residue was purified by FCC to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09265770B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-cd8ab399558b435a8402386ff664abf7 |
| Source note | uspto-grants-2016_02 |