HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(11-fluoro-6H-pyrido[2',3':5,6][1,3]oxazino[3,4-a]indol-2-yl)-2-(4-fluorophenyl)-6-(N-methylmethylsulfonamido)benzofuran-3-carboxamide → HCID 178464693, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(11-fluoro-6H-pyrido[2',3':5,6][1,3]oxazino[3,4-a]indol-2-yl)-2-(4-fluorophenyl)-6-(N-methylmethylsulfonamido)benzofuran-3-carboxamide | HCID 86728290 | — |
| Solvent | DMA dimethylacetamide | HCID 19097097 | — |
| Product | HCID 178464693 | HCID 178464693 | — |
Reaction Steps
To a solution of 5-(11-fluoro-6H-pyrido[2′,3′:5,6][1,3]oxazino[3,4-a]indol-2-yl)-2-(4-fluorophenyl)-6-(N-methylmethylsulfonamido)benzofuran-3-carboxamide (100 mg, 0.17 mmol) in DMA-DMA (2 mL) was stirred at 120° C. for 2 hour. The reaction mixture was concentrated in vacuo and the resulting residue was used to the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09265773B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-7a6b57e5fa0143a58a6302e47794454f |
| Source note | uspto-grants-2016_02 |