HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl oxoacetate → HCID 118201024, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl oxoacetate | HCID 70211 | — |
| Reactant | (2R)-1-aminopropan-2-ol | HCID 439938 | — |
| Reactant | 5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoic acid | HCID 53260165 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 118201024 | HCID 118201024 | — |
Reaction Steps
By using ethyl glyoxylate (polymer type, a solution of 47% toluene) (0.50 mL, 2.4 mmol), (2R)-1-aminopropan-2-ol (0.18 mL, 2.4 mmol) and 5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoic acid (0.20 g, 0.98 mmol), the same procedure as in Reference Example 1 was carried out to obtain the title compound (0.14 g) (colorless oil).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09266870B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-97267e7535564d7bb3587c43c1491ae9 |
| Source note | uspto-grants-2016_02 |