HCID 89726394, compound → HCID 59069112, compound

HRID 1777751Notes

Reaction equation

HRID 1777751 reaction equation
C([O:8][C:9](=[O:17])[CH2:10][N:11]1[CH:15]=[N:14][C:13]([CH3:16])=[N:12]1)C1C=CC=CC=1>CCO>[CH3:16][C:13]1[N:14]=[CH:15][N:11]([CH2:10][C:9]([OH:17])=[O:8])[N:12]=1

Participants

3

Reactant 1

HCID 89726394HCID 89726394, compound

Product 1

HCID 59069112HCID 59069112, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

This compound was prepared using a method analogous to that of Example 14 step 14.2, (3-methyl-[1,2,4]triazol-1-yl)acetic acid benzyl ester (described in Precursor for Example 212 step 212.1) replacing intermediate 14.1 and using EtOH instead of MeOH/AcOH. LC-MS (B): tR=0.18 min; [M+H]+: 142.22.

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-45f734e8b4214f6994279fa279948921
Source dataset
uspto-grants-2016_02
Patent number
US09266876B2

Reaction notes

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