HCID 89726306, compound → HCID 82585658, compound

HRID 1777756Notes

Reaction equation

HRID 1777756 reaction equation
C([O:8][C:9](=[O:21])[CH2:10][N:11]1[C:19]2[CH2:18][CH2:17][N:16]([CH3:20])[CH2:15][C:14]=2[CH:13]=[N:12]1)C1C=CC=CC=1>CO>[CH3:20][N:16]1[CH2:17][CH2:18][C:19]2[N:11]([CH2:10][C:9]([OH:21])=[O:8])[N:12]=[CH:13][C:14]=2[CH2:15]1

Participants

3

Reactant 1

HCID 89726306HCID 89726306, compound

Product 1

HCID 82585658HCID 82585658, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

This compound was prepared using a method analogous to that of Example 14 step 14.2, (5-methyl-4,5,6,7-tetrahydro-pyrazolo[4,3-c]pyridin-1-yl)-acetic acid benzyl ester (described in Precursor for Example 215) replacing intermediate 14.1 and using MeOH instead of MeOH/AcOH. LC-MS (B): tR=0.16 min; [M+H]+: 196.27.

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-fb55c00dae3749ef92c61f5d0bb3f986
Source dataset
uspto-grants-2016_02
Patent number
US09266876B2

Reaction notes

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