HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-ethyl 4-(tert-butoxycarbonyl)amino-5-methyl-3-oxohexanoate → HCID 118274919, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-ethyl 4-(tert-butoxycarbonyl)amino-5-methyl-3-oxohexanoate | HCID 13968762 | — |
| Reactant | 2-(tert-butoxycarbonylamino)-2-(tetrahydrofuran-3-yl)acetic acid | HCID 22309196 | — |
| Product | HCID 118274919 | HCID 118274919 | — |
Reaction Steps
Procedure same as that for ethyl(S)-4-((tert-butoxycarbonyl)amino)-5-methyl-3-oxohexanoate, using 2-((tert-butoxycarbonyl)amino)-2-(tetrahydrofuran-3-yl)acetic acid as a starting material. 1H NMR (CD3OD, 400 MHz): δ 4.25-4.13 (m, 3H), 4.00-3.45 (m, 4H), 2.75-2.65 (m, 1H), 2.12-1.98 (m, 1H), 1.77-1.62 (m, 1H), 1.49 (s 9H), 1.30 (t, J=7.2 Hz, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09266886B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-87bd35c23bb64d5cbda6ab5cc79a5e29 |
| Source note | uspto-grants-2016_02 |