HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Amino-4-chloro-3-pyridinecarbonitrile → HCID 118036729, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Amino-4-chloro-3-pyridinecarbonitrile | HCID 21949219 | — |
| Reactant | tert-Butyl 2,8-diazaspiro[4.5]decane-2-carboxylate | HCID 34178604 | — |
| Product | HCID 118036729 | HCID 118036729 | — |
Reaction Steps
From intermediate 16 and tert-butyl 2,8-diazaspiro[4.5]decane-2-carboxylate, reacted in an analogous manner to the preparation of intermediate 42. 1H NMR (400 MHz, DMSO-d6) δ 8.06 (s, 1H), 6.66 (s, 2H), 5.90 (s, 1H), 3.10-3.32 (s, 8H), 1.69-1.79 (m, 2H), 1.52-1.66 (m, 4H), 1.40 (s, 9H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09266883B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-95f7328154564306bac9fb6998a40dea |
| Source note | uspto-grants-2016_02 |