(R)-(-)-1-Methoxy-2-propanol → HCID 118036403, compound

HRID 1777952Notes

Reaction equation

HRID 1777952 reaction equation
COC[C@H](O)C.[Cl:7][C:8]1[N:13]=[C:12]([O:14][C@@H:15]([CH3:19])[CH2:16][O:17][CH3:18])[C:11]([Cl:20])=[CH:10][N:9]=1>>[Cl:7][C:8]1[N:13]=[C:12]([O:14][C@H:15]([CH3:19])[CH2:16][O:17][CH3:18])[C:11]([Cl:20])=[CH:10][N:9]=1

Participants

3

Reactant 2

HCID 2733589(R)-(-)-1-Methoxy-2-propanolHCID 118036789HCID 118036789, compound

Product 1

HCID 118036403HCID 118036403, compound

Procedure

From (R)-1-methoxypropan-2-ol, reacted in an analogous manner to the preparation of intermediate 91. (UPLC-MS 7) tR 1.02; ESI-MS 237.1 and 239.0 [M+H]+.

Sources & evidence

ORD record
ord-6b21ce6969d54c3daae97a35b81916e4
Source dataset
uspto-grants-2016_02
Patent number
US09266883B2

Reaction notes

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