HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Tolyl isocyanate → HCID 118130047, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Tolyl isocyanate | HCID 69303 | — |
| Reactant | Methyl 5-[N-({6-amino-5-[(3-aminophenyl)ethynyl]pyridin-3-yl}carbonyl)-S-methylsulfonimidoyl]pentanoate | HCID 118130063 | — |
| Product | HCID 118130047 | HCID 118130047 | — |
Reaction Steps
In a manner similar to that describe in Example 37, methyl 5-[N-({6-amino-5-[(3-aminophenyl)ethynyl]pyridin-3-yl}carbonyl)-S-methylsulfonimidoyl]pentanoate and 5-methylphenyl isocyanate were coupled. Purification of the crude reaction product gave the title compound as a white foam (78.8 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09266869B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-ed8486f5b0ec4196a5b870fef04e3e1d |
| Source note | uspto-grants-2016_02 |