Triacetoxyperiodinane → HCID 117706779, compound

Participants

Reaction Steps

0.8 g of nitrile 150b was dissolved in 10 ml of DCM. Then 3 eq of Dess-Martin reagent was added to the solution and stirred at room temperature overnight. The mixture was filtered and the filtrate was concentrated to give 8-benzyl-6-oxo-8-azabicyclo[3.2.1]octane-3-carbonitrile 150c as a crude product (0.9 g), which was used in the next step without further purification.

Provenance & Evidence