Isopropylamine → HCID 86722852, compound

HRID 1778755Notes

Reaction equation

HRID 1778755 reaction equation
[Br:1][C:2]1[C:11]([F:12])=[CH:10][C:5]([C:6]([O:8]C)=O)=[C:4]([CH2:13]Br)[CH:3]=1.[CH:15]([NH2:18])([CH3:17])[CH3:16]>>[Br:1][C:2]1[CH:3]=[C:4]2[C:5](=[CH:10][C:11]=1[F:12])[C:6](=[O:8])[N:18]([CH:15]([CH3:17])[CH3:16])[CH2:13]2

Participants

3

Reactant 2

HCID 6363IsopropylamineHCID 86722851Benzoic acid, 4-bromo-2-(bromomethyl)-5-fluoro-, methyl ester

Product 1

HCID 86722852HCID 86722852, compound

Procedure

This compound was prepared using procedures analogous to those described for the synthesis of Example 52, Step 6 starting from methyl 4-bromo-2-(bromomethyl)-5-fluorobenzoate and isopropylamine. LC/MS: (M+H)+=271.9/273.9.

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-13a36c8c52cf44b1b3cc7a4f0a22f092
Source dataset
uspto-grants-2016_02
Patent number
US09266892B2

Reaction notes

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