Diethylamine → HCID 21924212, compound

Participants

Reaction Steps

To 200 g of the acrylate obtained in Example 1.A, 18.6 g of diethylamine was added in order to reach in the end product, a nitrogen content of 1.2%. After the slight exotherm observed during addition of the amine, the reaction mixture was maintain at 50° C. until the free diethylamine content reached 1000 ppm, as measured by titration. After being stripped to reach a free diethylamine content below 200 ppm, the end product was post-stabilized with 3000 ppm trisnonylphenylphosphite. A clear, low odour, low viscous (viscosity C/P (25° C.)=172 mPa·s) and low colored (0.8 Gardner) product was obtained.

Provenance & Evidence