HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86681298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Bromopyrazole | HCID 16375 | — |
| Reactant | Bromodiphenylmethane | HCID 236603 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86681298 | HCID 86681298 | — |
Reaction Steps
A solution of 4-bromo-1H-pyrazole (0.294 g), (bromomethylene)dibenzene (0.494 g) and triethylamine (0.418 mL) in tetrahydrofuran (5 mL) was stirred at 60° C. for 24 hours. The reaction mixture was concentrated and purified by chromatography on silica gel using 0-20% ethyl acetate/hexanes as eluent to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09266877B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-9d0bfc5c94284c248f6c532b1ba5f6a0 |
| Source note | uspto-grants-2016_02 |