HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Isobutylene → N-(2,6-diethylphenyl)maleimide isobutene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Isobutylene | HCID 8255 | — |
| Edukt | 1-(2,6-diethylphenyl)-1H-pyrrole-2,5-dione | HCID 300890 | — |
| Edukt | Neodecanoate | HCID 21225528 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | N-(2,6-diethylphenyl)maleimide isobutene | HCID 68407703 | — |
Reaktionsschritte
Into a 1-liter autoclave were introduced 400 mL of toluene as a polymerization solvent, 0.001 mol of perbutyl neodecanoate as a polymerization initiator, 0.42 mol of N-(2,6-diethylphenyl)maleimide, and 4.05 mol, of isobutene. A polymerization reaction was conducted at a polymerization temperature of 60° C. for a polymerization time of 5 hours to obtain an N-(2,6-diethylphenyl)maleimide-isobutene alternating copolymer. The N-(2,6-diethylphenyl)maleimide-isobutene alternating copolymer obtained had a number-average molecular weight of 65,000.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09268076B2 |
| Quelldatensatz | uspto-grants-2016_02 |
| ORD ID | ord-844aaebf1892438a830d53ac5fd8ccea |
| Quellennotiz | uspto-grants-2016_02 |