HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 131734842, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | Sulfur trioxide | HCID 24682 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Hexane | HCID 8058 | — |
| Solvent | Heptane | HCID 8900 | — |
| Product | HCID 131734842 | HCID 131734842 | — |
Reaction Steps
To 1.34 g of imidazole in suspension in heptane is added 1 ml of 2M butyllithium in hexane and the mixture is stirred at room temperature for 24 hours. To this suspension, are added 3.2 g of sulfur trioxide in dichloromethane. The slurry is stirred further for 24 hours and the solids are separated by centrifugation to yield lithium [1,3 disulfonatoimidazolium].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09269987B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-45e071df2c5b4a8c8a4aa53ab5462496 |
| Source note | uspto-grants-2016_02 |