HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethynylphenol → HCID 131720003, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethynylphenol | HCID 32758 | — |
| Reactant | Benzyl isopropenyl ether | HCID 560989 | — |
| Product | HCID 131720003 | HCID 131720003 | 62.3% |
Reaction Steps
Using poly(p-hydroxystyrene) (4.0 g) [available from Maruzen Petrochemical Co., Ltd.: Mw ca. 20000] and benzylisopropenylether (4.2 g) [purchased from Tokyo Chemical Industry Co., Ltd.], the reaction and treatment were carried out in the same manner as described in Synthesis Example 2, to give 4.1 g of the desired product as a slightly yellow powder. The polymer was found to have p-(1-benzyloxy-1-methylethoxy)styrene unit and p-hydroxystyrene unit in a molar ratio of 4:6 based on 1HNMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05627006 |
| Source dataset | uspto-grants-1997_05 |
| ORD ID | ord-d32d76e64a2f48d5913432b2df919d0d |
| Source note | uspto-grants-1997_05 |