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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1779347Generated: October 31, 2026

Oxalyl chloride → 3,4,4-Trifluoro-3-butenoyl chloride

https://huagongshe.com/reaction/1779347

Reaction equation

Participants

RoleNameHCIDCharge
ReactantOxalyl chlorideHCID 65578—
Reactant3,4,4-Trifluoro-3-butenoic acidHCID 15239174—
CatalystDimethylformamideHCID 6228—
Product3,4,4-Trifluoro-3-butenoyl chlorideHCID 10920789—

Reaction Steps

Reaction of 3,4,4-trifluoro-3-butenoic acid (IV) with oxalyl chloride in the presence of DMF as a catalyst without any solvent to give 3,4,4-trifluoro-3-butenoyl chloride (V).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05627174
Source datasetuspto-grants-1997_05
ORD IDord-714a95f1de3f4a48ba5c6a26a4a974f1
Source noteuspto-grants-1997_05