HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10565709, compound → HCID 22872473, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10565709 | HCID 10565709 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 22872473 | HCID 22872473 | — |
Reaction Steps
To a solution of methyl 2(S)-benzyloxycarbonylamino-3-acetylamino-propionate (2.2 g ) in ethanolic HCl was added 10% Pd/C(0.3 g) under nitrogen atmosphere. Hydrogen was applied to the mixture at 60 psi for 16 h. The mixture was filtered and concentrated in vacuo. The residue was triturated with diethyl ether to obtain the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05627202 |
| Source dataset | uspto-grants-1997_05 |
| ORD ID | ord-0fb5c0857b6b499da8f9e9594eedc2d0 |
| Source note | uspto-grants-1997_05 |